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The XRD results confirmed the same influence of ligand molecule and activity of Se source on the phase of synthesized NCs (Supplementary Figure S3). From the above control experiments, it can be concluded that the strong ligands promote the decomposition of metal compounds and are favored for reducing surface energy, and high activity of the Se source provides high reaction rate, which together make the dynamically stable products dominant. High reaction rate and low surface energy are indispensable for CZTSe NCs with a thermodynamically metastable wurtzite structure..
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